Tellurium in Organic Synthesis 2nd Edition by Nicola Petragnani, Helio Stefani ISBN 0080453104 9780080453101

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ISBN 10: 0080453104 
ISBN 13: 9780080453101
Author: Nicola Petragnani, Helio Stefani

The increasing number of publications that use tellurium clearly demonstrates the important role of tellurium compounds as unique and powerful tools in a broad range of organic chemical manipulations, often characterized by their selective behavior.
Tellurium in Organic Synthesis provides an overview of the principal aspects of organic tellurium chemistry. Many chapters have been enriched and updated in this second edition. New chapters include overviews of toxicology and pharmacology and a review on the preparation and reactivity of several tellurium heterocycles.
The first part of the book focuses on the preparation of selected inorganic tellurium compounds and on the main classes of organotellurium compounds. The second part, and main interest of the book, details the use of these inorganic and organic compounds as reagents to perform specific organic manipulations and synthesis. Reactions covered include reduction, formation and reaction of anionic species, deprotection, tellurium cyclizations, formation of alkenes, use of vinyllic tellurides, free radical chemistry, transmetallations, and removal of tellurium.

* Overview of inorganic and organic tellurium chemistry
* Synthetic applications of tellurium compounds
* All topics accompanied by detailed experimental procedures

Tellurium in Organic Synthesis 2nd Table of contents:

Chapter 1: Introduction
Publisher Summary
1.1 SOME PHYSICAL PROPERTIES OF TELLURIUM
Chapter 2: Preparation of the More Important Inorganic Tellurium Reagents
Publisher Summary
2.1 TELLURIUM TETRACHLORIDE
2.2 TELLURIUM DIOXIDE
2.3 ALKALI METAL TELLURIDES (Te2−Cat2+)
2.4 ALKALI METAL DITELLURIDES (Na2Te2)
2.5 HYDROGEN TELLURIDE (H2Te)
2.6 SODIUM HYDROGEN TELLURIDE (NaHTe)
Chapter 3: Preparation of the Principal Classes of Organic Tellurium Compounds
Publisher Summary
DIORGANYL TELLURIDES (SECTION 3.1)
DIORGANYL DITELLURIDES (SECTION 3.2)
ORGANYLTELLURIUM TRICHLORIDE AND DIORGANYLTELLURIUM DIHALIDES (SECTIONS 3.5 AND 3.9)
3.1 DIORGANYL TELLURIDES
3.1.2 Symmetrical diaryl tellurides
3.1.3 Unsymmetrical tellurides
3.1.4 Diorganyl tellurides by reduction of diorganyltellurium dihalides
3.1.5 Additional methods
3.2 DIORGANYL DITELLURIDES
3.3 ORGANYL TELLUROLS
3.4 BIS-ORGANYL TELLUROMETHANES
3.5 ORGANYLTELLURIUM TRIHALIDES
3.6 THE PRODUCTS OF THE HYDROLYSIS OF ARYLTELLURIUM TRIHALIDES
3.7 ARYLTELLURENYL HALIDES
3.8 ARYL TELLURENYL PSEUDOHALIDES: ARYL TELLUROCYANATES
3.9 DIORGANYL TELLURIUM DIHALIDES
3.10 DIORGANYL TELLUROXIDES
3.11 TELLUROESTERS
3.12 ARYL TELLUROFORMATES
3.13 TELLUROGLUCOPYRANOSIDES
3.14 WATER-SOLUBLE DIORGANYL TELLURIDES
3.15 DIHALOARYLTELLURO CYCLOPROPANES
3.16 VINYLIC TELLURIDES AND DITELLURIDES
3.17 ACETYLENIC TELLURIDES
3.18 ALLENIC AND PROPARGYLIC TELLURIDES
Chapter 4: Tellurium in Organic Synthesis
Publisher Summary
4.1 REDUCTIONS
4.2 TELLURIUM-MEDIATED FORMATION OF ANIONIC SPECIES AND THEIR REACTIONS WITH ELECTROPHILES
4.2.7 Miscellaneous
4.3 DEPROTECTION OF ORGANIC FUNCTIONALITY BY TELLURIUM REAGENTS
4.4 OXIDATION OF ORGANIC SUBSTANCES BY MEANS OF TELLURIUM REAGENTS
4.5 ORGANOTELLURIUM-BASED RING CLOSURE REACTIONS
4.6 CONVERSION OF ORGANOTELLURIUM COMPOUNDS INTO TELLURIUM-FREE ORGANIC COMPOUNDS
4.7 SYNTHESIS OF OLEFINS
4.8 TRANSMETALLATION REACTIONS
4.9 REACTIVITY AND SYNTHETIC APPLICATIONS OF VINYLIC TELLURIDES
4.10 FREE RADICAL CHEMISTRY
Chapter 5: Telluroheterocycles
Publisher Summary
5.1 TELLURA-3,5-CYCLOHEXANEDIONE DICHLORIDES (3,5-DIOXOTELLURANE-1,1-DICHLORIDES)
5.2 OXA AND 1-THIA-4-TELLURANES
5.3 TELLUROPHENES
5.4 1-BENZOTELLUROPHENES
5.5 BENZOTELLUREPINES, TELLUROCHROMENES AND TELLUROCHROMONES
5.6 BENZO-[c]-TELLUROPHENES
5.7 TELLURO[3,4-c]THIOPHENE
5.8 DIBENZOTELLUROPHENES
5.9 NAPHTOTHIA-, NAPHTOSELENA- AND NAPHTODITELLUROLE
5.10 2H-1,3-DITELLUROLES
5.11 TETRATELLURAFULVALENES
5.12 TELLURIN AND DERIVATIVES OF 4-H-TELLURINS AND 4-OXO-4-H-TELLURINS (TELLUROPYRAN-4-ONES)
5.13 2H-1-BENZOTELLURIN
5.14 4H-1-BENZOTELLURINS AND 4-OXO-4H-1-BENZOTELLURINS
5.15 TELLUROXANTHENES/TELLUROXANTHONES (AND DERIVATIVES)
5.16 PHENOXATELLURINS
5.17 PHENOTHIATELLURINS/PHENOSELENOTELLURINS
5.18 TELLURANTHRENES
5.19 BIS-THIENO-1,4-DITELLURINS
5.20 1,4-TELLURINO-1,4-TELLURINS
5.21 BENZENE-FUSED HETEROCYCLES CONTAINING TELLURIUM, SELENIUM AND SULPHUR
5.22 1,5-DITELLURACYCLOOCTANE AND 5H,7H-DIBENZO[b,g][1,5] TELLUROTHIOCIN
5.23 DITELLURANE DERIVATIVES
5.24 REDUCTIVE DIMERIZATION OF TELLURO- AND SELENOXANTHONE
Chapter 6: Toxicology of Organotellurium Compounds
Publisher Summary
Chapter 7: Pharmacology of Organotellurium Compounds
Publisher Summary
7.1 CHEMOPREVENTIVE ACTIVITY
Chapter 8: Miscellaneous
Publisher Summary
8.1 SOME ADDITIONAL APPLICATIONS OF TeCl4
8.2 α-HYDROXYALKYLATION OF α,β-UNSATURATED CARBONYL COMPOUNDS
8.3 CONVERSION OF ALLYLSILANES INTO ALLYLAMINES VIA PHENYLTELLURINYLATION

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Nicola Petragnani,Helio Stefani,Tellurium,Organic Synthesis