NMR Spectroscopy Data Acquisition 2nd Edition by Christian Schorn, Brian J. Taylor – Ebook PDF Instant Download/Delivery: 3527310703, 9783527310708
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Product details:
ISBN 10: 3527310703
ISBN 13: 9783527310708
Author: Christian Schorn, Brian J. Taylor
The key to correct structure analysis now in its second edition.
There have been many important advances in the field since the first publication of this book. Consequently, this edition has been extended to incorporate a number of pulse sequence developments. Nevertheless, it still details the basic experiments on a step-by-step basis, such that students and newcomers may come to understand basic data acquisition procedures, modular pulse sequence units, and complete sequences in NMR spectroscopy. The author applies the numerous possibilities of Bruker’s simulation program NMR-SIM to provide a guided introduction to the world of pulse sequences. The effectiveness of particular NMR experiments is demonstrated by the “Check Its” section and that of data processing by the accompanying CD-ROM containing the Bruker processing software 1D and 2D WIN-NMR.
Major revisions include increased coverage of simulations of multiple offset selective pulse experiments as well as filter elements. One new chapter is a collection of some of the latest published ideas to improve existing sequences, together with spin-state selective experiments.
The result is a volume encouraging beginners to use high resolution NMR, while prompting experts to evaluate new experiments using the easy-manageable simulation program.
NMR Spectroscopy Data Acquisition 2nd Table of contents:
Chapter 1: Introduction to NMR Spectroscopy
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Basic Principles of NMR
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Historical Overview
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Applications of NMR Spectroscopy
Chapter 2: The NMR Spectrometer
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Components of an NMR Spectrometer
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Magnet Technology
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Radiofrequency Coils and Probes
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Gradient Systems
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Data Acquisition Hardware and Software
Chapter 3: Pulse Sequences and Basic Experiments
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Continuous Wave vs. Fourier Transform NMR
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Common Pulse Sequences
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Single Pulse Experiment
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Spin Echo and Inversion Recovery
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Saturation and Decoupling Techniques
Chapter 4: Data Acquisition Parameters
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Spectral Width and Resolution
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Sampling and Digital Resolution
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Relaxation Times and Their Effect on Data
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Signal Averaging and Sensitivity
Chapter 5: Advanced Acquisition Techniques
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Multidimensional NMR Experiments
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Techniques for Sensitivity Enhancement
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Fast Acquisition Methods
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Non-Uniform Sampling
Chapter 6: Data Processing and Interpretation
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Fourier Transformation
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Phase Correction
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Baseline Correction
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Integration and Peak Picking
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Quantitative NMR
Chapter 7: Troubleshooting and Optimization
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Common Problems in Data Acquisition
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Optimization of Pulse Parameters
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Artifacts and Their Elimination
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