Multinuclear Solid State NMR of Inorganic Materials 1st Edition by Kenneth Mackenzie, Mark Smith ISBN 9780080537108, 0080537103
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ISBN 10: 0080537103
ISBN 13: 9780080537108
Author: Kenneth Mackenzie, Mark Smith
Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments.
With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.
Multinuclear Solid State NMR of Inorganic Materials 1st Edition Table of contents:
Chapter 1. Introduction
1.1. Methodology of Materials Characterisation by NMR
1.2. Historical Aspects of NMR Spectroscopy
1.3. Brief Description of the NMR Experiment
1.4. Further Reading
References
Chapter 2. Physical Background
2.1. Fundamental Interaction with External Magnetic Fields
2.2. Internal Interactions
2.3. One Dimensional Methods for Improving Resolution
2.4. Dipolar Decoupling
2.5. Spin-locking
2.6. Cross-Polarisation
2.7. Two-Dimensional Methods
2.8. NMR Relaxation
References
Chapter 3. Experimental Approaches
3.1. Basic Experimental Principles of FT NMR
3.2. Instrumentation
3.3. Practical Acquisition of NMR Spectra
3.4. Static Broad Line Experiments
3.5. One-Dimensional High Resolution Techniques
3.6. Two-Dimensional Experiments
3.7. Summary of Approaches for Examining Quadrupole Nuclei
3.8. Multiple Resonance
3.9. Techniques for Determining Relaxation Times and Motional Parameters
3.10. NMR Under Varying Physical Conditions
References
Chapter 4. 29Si NMR
4.1. General Considerations
4.2. Si-O Compounds
4.3. Order-Disorder Effects in Minerals
4.4. Identification of Silicate Minerals
4.5. Thermal Decomposition of Silicate Minerals
4.6. Relationships between 29Si Chemical Shift (δ) and Structure
4.7. Five and Six-Coordinated Si-O Compounds
4.8. Cross-Polarisation (CPMAS) Experiments
4.9. Glasses, Gels and Other Amorphous Materials
4.10. Si-N and Si-N-O Compounds
4.11. Si-AL-O-N Compounds
4.12. Other Metal Silicon Nitrides and Oxynitrides
4.13. Si-C, Si-C-O and Si-C-N Compounds
4.14. Other Materials
References
Chapter 5. 27AL NMR
5.1. General Considerations
5.2. Chemical Shifts in 27Al Spectra
5.3. Five-Coordinated Al-O
5.4. Aluminium Oxides
5.5. Amorphous Aluminium Compounds
5.6. Aluminophosphates
5.7. Aluminium Borate and Molybdate
5.8. Aluminium Fluorides
5.9. Thermal Decomposition Reactions
5.10. Cements
5.11. Nitride and Oxynitride Compounds
5.12. Sialon Compounds
References
Chapter 6. 17 O NMR
6.1. Introduction
6.2. Background
6.3. Binary Oxides
6.4. Crystalline Ternary Ionic Systems
6.5. Silicates and Germanates
6.6. Aluminium- and Gallium-Containing Systems
6.7. Boron-Containing Systems
6.8. Other Systems
6.9. Hydrogen-Containing Samples
6.10. High Temperature Ceramic Superconductors
References
Chapter 7. NMR of Other Commonly Studied Nuclei
7.1. 23Na NMR
7.2. 11B NMR
7.3. 31P NMR
References
Chapter 8. NMR of Low-γ Nuclides
8.1. General Considerations
8.2. NMR of Spin-1/2 Nuclei
8.3. Quadrupolar Nuclei
References
Chapter 9. NMR of Other Spin-1/2 Nuclei
9.1. Introduction
9.2. Abundant High-γ Nuclei
9.3. Dilute or Medium-γ Nuclei
References
Chapter 10. NMR of Other Quadrupolar Nuclei
10.1. 6Li and 7Li NMR
10.2. 9Be NMR
10.3. 51V NMR
10.4. 63Cu and 65Cu NMR
10.5. 69Ga and 71Ga NMR
10.6. 87Rb NMR
10.7. 93Nb NMR
10.8. 133Cs NMR
10.9. 139La NMR
References
Chapter 11. Solid State NMR of Metals and Alloys
11.1. Introduction
11.2. Experimental Approaches
11.3. Metallic Elements
11.4. Intermetallic Alloys
11.5. Phase Transformations, Ordering and Defect Sites
11.6. Phase Composition and Precipitation
11.7. Atomic Motion
References
Subject Index
Mineral Index
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