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Heterophase network polymers synthesis characterization and properties 1st Edition by Boris Aleksandrovich Rozenberg, Grigori M Sigalov ISBN 0415284171 9780415284172

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Heterophase network polymers synthesis characterization and properties 1st Edition Boris Aleksandrovich Rozenberg Digital Instant Download

Author(s): Boris Aleksandrovich Rozenberg, Grigori M. Sigalov
ISBN(s): 0415284171
Edition: 1
File Details: PDF, 5.15 MB
Year: 2002
Language: english
SKU: EB-2120394 Category: Tags: ,

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ISBN 10: 0415284171 
ISBN 13: 9780415284172
Author: Boris Aleksandrovich Rozenberg, Grigori M Sigalov

This volume explains the theory and experimental investigations in the preparation of heterophase polymer network materials through cure reaction-induced microphase separation (CRIMPS). It describes the synthesis of a new family of block- and graft-copolymers with controlled solubility in epoxies and characterizes CRIMPS processes using novel applications of known methods such as nuclear magnetic resonance, electron spin resonance and photochemistry. The text develops a new method for characterizing the molecular mass distribution (MMD) of linear and network polymers using thermomechanical analysis data, as well as new methods for determining internal stresses and flaw formation during thermoset curing. The CRIMPS theory will be helpful for researchers and engineers designing and improving toughened plastics and other smart heterophase network materials for different applications. The new method for MMD characterization of polymers in bulk will be very useful to quickly analyze a polymer’s MMD and to design new polymers. This book will provide a useful reference for graduates, researchers and working professionals in polymer chemistry and physics and materials science.

Heterophase network polymers synthesis characterization and properties 1st Table of contents:

I. Synthesis and Characterization of Modifiers

  • Ch 1: Synthesis of bifunctional oligobutadienes initiated by dilithium alkanes

  • Ch 2: Block copolymers with controlled solubility in epoxy resins

  • Ch 3: Universal calibration in gel permeation chromatography

  • Ch 4: Phase equilibrium in binary polymer systems (diglycidyl ether of bisphenol A)

II. Theory of Microphase Separation in Curing Systems

  • Ch 5: Cure reaction-induced microphase separation (nonequilibrium nucleation and growth)

  • Ch 6: Analytical description of microphase formation in curing blends

  • Ch 7: 2D model of phase separation during polymerization of binary polymer blends

  • Ch 8: Theory and simulation for dynamics of polymerization-induced phase separation

  • Ch 9: Phase diagrams of multicomponent reacting polymer systems

III. Kinetics and Mechanism of Cure Reactions and Reaction-Induced Microphase Separation

  • Ch 10: Cure rate and CRIMPS mechanism

  • Ch 11: Role of intermolecular interactions in polyurethane formation

  • Ch 12: Formation of spatial dissipative structures during polyurethane synthesis

IV. Structure–Properties Relationship

  • Ch 13: Thermoset/thermoplastic blends with crosslinked thermoplastic network

  • Ch 14: Epoxy-based PDLCs: formation, morphology, electrooptical properties

  • Ch 15: Crosslinking studies in rigid and semi-rigid polymers

  • Ch 16: Modeling shrinkage defects in fiber composites

  • Ch 17: Analysis of shrinkage cracking in 3D constrained heterophase polymers

  • Ch 18: Modeling polymer film formation by spin coating

  • Ch 19: Thermal decomposition of thin polyepoxide films

V. New Approaches to Polymer Networks Characterization

  • Ch 20: Characterization of molecular weight distribution for linear and network polymers

  • Ch 21: Microphase separation in epoxies studied by photoactive probe technique

  • Ch 22: Investigation of CRIMPS by NMR

  • Ch 23: CRIMPS in epoxy-amine system studied by ESR

  • Ch 24: Gelation and reaction-induced microphase separation studied by dielectroscopy

  • Ch 25: Pulsed NQR for measuring internal stresses in polymers and composites

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Tags: Boris Aleksandrovich Rozenberg, Grigori M Sigalov, Heterophase network, synthesis characterization